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I am not close to being a professional at making biodiesel, but I have yet to fail a 3/27 test. Here are a few things I have seen cause a failure. Make sure you TRUST your container markings. I have seen may people use a container and add 30 gallons to the mark to find out they have unreacted fuel because the mark was WRONG and they had 31-32 gallons. If you are making a 30 gallon batch this means 30 gallons, not 30 gallons pump and hoses full of oil. Make sure you have your oil heated to 130 degrees before mixing the Methanol Mix. Use a PUMP! People have been on here saying they are trying to stir mix the batch together which will take forever and is also DANGEROUS! You don't want to be exposed to fumes, period. Your time of mixing matters. I mix a 30 gallon batch at 135-138 degrees for 2 hours. Get a temp gauge built in so you can watch what is really going on. Learn how to do good titration tests. This will make a big difference in SOAP problems.


2006 Dodge Ram 2500 5.9L Turbo Diesel

Fuel Blends, Recorded Miles
Diesel: 30194
B20: 978
B40: 447
B60: 2167
B80: 1673
B100: 1239
 
Location: Southern Minnesota | Registered: 01 March 2008Reply With QuoteEdit or Delete MessageReport This Post
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Hello hiperf2007
quote:
Originally posted by hiperf2007:
Use a PUMP! People have been on here saying they are trying to stir mix the batch together which will take forever and is also DANGEROUS!
The BioPro seems to be quite safe and it uses stir mixing.
Most reactors that uses a pump for mixing seem to use a poor quality pump that was not designed to pump caustic chemicals and has a history of failing and catching fire.


Saint Tilly



 
Location: ลึก ประเทศอินเดีย | Registered: 03 March 2001Reply With QuoteEdit or Delete MessageReport This Post
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hiper

you failed to mention about water testing and dewatering as well as the importance of getting food/batter chunkies completely out.

I mention this because there have been no less than 20 people or so in the last month who have had messed up batches and/or emulsions because of excess water.

On the subject of pumps. It is not terribly expensive to purchase a 1 hp motor - they can be had for about 85 dollars and a gear pump - can be had for under 200 dollars.

I realize that's more than the 30 or 35 bucks that people pay for the harbor freight jobbie, but given the cost of diesel right now and the amount saved per batch it only takes 1 or 2 batches to pay for a far superior setup. Which will result in greater reliability as well as better mixing which will aid the process.
 
Registered: 20 May 2008Reply With QuoteEdit or Delete MessageReport This Post
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Use two Clear Water Pumps in parallel. Much less expensive than other pump options, and it will most likely eliminate the over amping reliability problem during mixing.
 
Location: Possum Lake Lodge, Canukland | Registered: 03 May 2005Reply With QuoteEdit or Delete MessageReport This Post
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It could also be mentioned that just searching through the archives will likely reveal the answer. Doing a little leg/ finger work goes a long way.
 
Location: central virginia | Registered: 13 March 2008Reply With QuoteEdit or Delete MessageReport This Post
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Hello John
quote:
Originally posted by john galt:
Use two Clear Water Pumps in parallel. Much less expensive than other pump options, and it will most likely eliminate the over amping reliability problem during mixing.
Can you please explain how hooking two Clear Water pumps in Parallel will "eliminate the over amping reliability problem during mixing"


Saint Tilly



 
Location: ลึก ประเทศอินเดีย | Registered: 03 March 2001Reply With QuoteEdit or Delete MessageReport This Post
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quote:
Originally posted by Tilly:
Hello hiperf2007
quote:
Originally posted by hiperf2007:
Use a PUMP! People have been on here saying they are trying to stir mix the batch together which will take forever and is also DANGEROUS!
The BioPro seems to be quite safe and it uses stir mixing.
Most reactors that uses a pump for mixing seem to use a poor quality pump that was not designed to pump caustic chemicals and has a history of failing and catching fire.


Tilly,
I am talking about the people that try to do this in a 5 gallon bucket and a wood stick. Some people might try and jump into this to fast and get blown up.. Just some things to think about and yes, the wood stick has been done. I have people PM me asking my why that was not working... Roll Eyes
I should of added there are TONS of forums on this site explaining anything and everything you could want to know, but the far best is all the people here to help and response to questions. You guys rock. Big Grin


2006 Dodge Ram 2500 5.9L Turbo Diesel

Fuel Blends, Recorded Miles
Diesel: 30194
B20: 978
B40: 447
B60: 2167
B80: 1673
B100: 1239
 
Location: Southern Minnesota | Registered: 01 March 2008Reply With QuoteEdit or Delete MessageReport This Post
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Hello hiperf2007
quote:
Originally posted by hiperf2007:
Tilly,
I am talking about the people that try to do this in a 5 gallon bucket and a wood stick. Some people might try and jump into this to fast and get blown up. Just some things to think about and yes, the wood stick has been done.
Oh, you mean David Hill'sWorld Famous Flat Stick Technique (Pat Pend)Yes, that has been around about as long as the World Famous Dr Pepper Technique (Pat Pend)
He used to do production batches in a cement mixer but one day he had to leave his cement mixer on the job and the last I knew Dave had upsized his World Famous Flat Stick Technique (Pat Pend) and reacts in a 200 litre drum mixing with a 1X2 flat Stick.

By the way, can you think of a reason why two Water Pumps in parallel will "eliminate the over amping reliability problem during mixing"
It does not add up to me.


Saint Tilly



 
Location: ลึก ประเทศอินเดีย | Registered: 03 March 2001Reply With QuoteEdit or Delete MessageReport This Post
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quote:
why two Water Pumps in parallel will "eliminate the over amping reliability problem during mixing"


This has been discussed in detail before on this forum and is also available through Google. Two pumps in parallel share the load and increase the flow or head as much as 30% depending on the pump curves and the operating head.

It's a common practice in the HVAC industry, and avoids the problem of oversized pumps for intermittent high viscosity loads, or when higher flow is needed for heating at extreme cold temperatures. It also provides a standby pump should one fail.
 
Location: Possum Lake Lodge, Canukland | Registered: 03 May 2005Reply With QuoteEdit or Delete MessageReport This Post
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Flat stick in an OPEN barrel????

I am not saying it won't work.

What was his methanol exposure?

Granted, I think the "methanol exposure" phobia is over rated. However, mixing hot oil with methoxide in an open top barrel.... well.... Did he ever talk about his headaches or blurred vision?


.

C.


Pump and Heater controllers are a must have. (ask Tilly why)
2006 - Jeep Liberty CRD - Wife drives -
1983 - Mercedes 300SD - Veggie experiment car "Casper"
2006 - Toyota Sienna - Mine :-( Hey, it's a comapny car!
 
Location: New England | Registered: 16 July 2005Reply With QuoteEdit or Delete MessageReport This Post
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Hmm so you "pump" 35gall (I guess that is US galls so in real talk it is 130 Ltrs) for 2hrs at 135 degress (read approx 57 Deg C).. Two things jump out at Me here !. most of the failed batches and problem batches I see on here are in the "appleseed " type reactors and usually are the result of under mixing ..ie the use of pump to mix ..and 2. at 57 deg C if you were to MIX ie stir you only have to stir for approx 50 mins hence a huge waste of energy. I agree care has to be taken and a properly designed plant that has a stir rather than a pump to mix is as safe as the appleseed design. It would appear the only real reason for a closed system like an appleseed is so higher presures therefore higher temps there fore less mixing time is required The plant I have is closed (no not sealed ) and I process at 55 deg for 45 Mins and also pass 3/27 test religiously ... the point of My comment is ... there is NOT a single way that is the best to process ..it just depends on the things you wish to gain from the bio experience ..personally I wish to make cheek GOOD fuel safely and to be aware of energy and enviroment concerns ...regards Kev
 
Location: West Australia | Registered: 20 November 2005Reply With QuoteEdit or Delete MessageReport This Post
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Hello John
quote:
Originally posted by john galt:
This has been discussed in detail before on this forum and is also available through Google.
Can you give me a link to where this has been discussed n this forum, I have had a look and can not find it.
quote:
Two pumps in parallel share the load and increase the flow or head as much as 30% depending on the pump curves and the operating head.
Do you mean that 2 pumps would only result in a 30% increase in flow rate compared to a single pump?
It would seem to me that as there is no controller on the pump, each pump would continue to run as normal and the only reason you would not be pumping twice the volume is if it were constricted by the size of the delivery or discharge pipe, And in some situations this could result in overheating.
Or do you mean that there will be double the flow rate plus 30%?
quote:
It's a common practice in the HVAC industry, and avoids the problem of oversized pumps for intermittent high viscosity loads, or when higher flow is needed for heating at extreme cold temperatures.
Do you feel this applies to biodiesel production in most situations? If you do, Can you explain where and when this would be applicable for biodiesel production
quote:
It also provides a standby pump should one fail.
As most of the overheat/fire problems seem to occur when the capacitor blows or the rotor jams do you think a second pump would have any affect on the temperature of the failed pump?


Saint Tilly



 
Location: ลึก ประเทศอินเดีย | Registered: 03 March 2001Reply With QuoteEdit or Delete MessageReport This Post
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This should answer your questions. I found the link, and here's the message.

Parallel pumps with check valves to prevent back flow are quite common in commercial applications


http://www.bellgossett.com/Press/BG-unparallel.asp

As the graph shows, flow will increase by about 112% and head (pressure) will increase by about 140% in the example shown. Specific applications will vary.

The caps on the CW pumps fail because the pumps frequently push their amp limits when starting to mix thick VO while it's reacting with methoxide or starting with cold VO. Running two in parallel during these stages would likely significantly extend pump life and reduce the over-amp overheating problem.
 
Location: Possum Lake Lodge, Canukland | Registered: 03 May 2005Reply With QuoteEdit or Delete MessageReport This Post
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Hello John
quote:
Originally posted by john galt:
This should answer your questions. I found the link, and here's the message.
Can you provide the link to the thread.
Is the graph you have displayed to the HF clearwater pump?


Saint Tilly



 
Location: ลึก ประเทศอินเดีย | Registered: 03 March 2001Reply With QuoteEdit or Delete MessageReport This Post
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quote:
As most of the overheat/fire problems seem to occur when the capacitor blows or the rotor jams do you think a second pump would have any affect on the temperature of the failed pump?

Just to clarify...
In the case of the HF pump, the capacitor is a start capacitor and can blow or even be removed while the pump is running with no ill effect to the pump... It will just not start again without some help...
Jon
 
Location: Wellington County, Ontario Canada | Registered: 07 February 2008Reply With QuoteEdit or Delete MessageReport This Post
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quote:
Originally posted by Jon Heron:
quote:
As most of the overheat/fire problems seem to occur when the capacitor blows or the rotor jams do you think a second pump would have any affect on the temperature of the failed pump?

Just to clarify...
In the case of the HF pump, the capacitor is a start capacitor and can blow or even be removed while the pump is running with no ill effect to the pump... It will just not start again without some help...
Jon


.......... or, may start turning in the oppsite direction no? Starter caps have a + and a - to them so they "push" the windings in the proper direction.


.

C.


Pump and Heater controllers are a must have. (ask Tilly why)
2006 - Jeep Liberty CRD - Wife drives -
1983 - Mercedes 300SD - Veggie experiment car "Casper"
2006 - Toyota Sienna - Mine :-( Hey, it's a comapny car!
 
Location: New England | Registered: 16 July 2005Reply With QuoteEdit or Delete MessageReport This Post
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Carl,
No this is incorrect. The start caps on an AC motor are not polarized(+ or -) If a DC cap is used you will be in for a big surprise... BANG.!!!
Once the motor starts turning the Start Capacitor has no effect whatsoever... Its strictly to start the motor.
In laymen terms the capacitor provides a delay in the power given to one of the windings. This delay causes the magnetic forces of the motor to be unbalanced and the motor then starts to turn in the direction of the weakest pole.
Jon
 
Location: Wellington County, Ontario Canada | Registered: 07 February 2008Reply With QuoteEdit or Delete MessageReport This Post
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quote:
Originally posted by RNCarl:
Flat stick in an OPEN barrel????

I am not saying it won't work.

What was his methanol exposure?

Granted, I think the "methanol exposure" phobia is over rated. However, mixing hot oil with methoxide in an open top barrel.... well.... Did he ever talk about his headaches or blurred vision?


Tilly,

You never commented on this post.

Isn't there someone else that has a "canoe paddle" method (pat. pending) that mixes like less than 15 min???

Physical agitation is the best way to get the little molecules striking into each other.

So, why not pump, yes pump the oil through an inline heater (static mixer) and introduce the methoxide via venturi (high surface area ratio due to the small(ish) volume of oil speeding through the narrow passage; Then splash it into the tank where it is sucked through the pump and forcesd through the static mixer (heating element) on its way once again to be bombarded again with the methoxide through the venturi.

Or, dump the methoxide into an open 55 gallon drum that contains your heated oil, mix it with a canoe paddle for 15 min or so, get a headache, have a few beers to make the headache go away and call it a day...


.

C.


Pump and Heater controllers are a must have. (ask Tilly why)
2006 - Jeep Liberty CRD - Wife drives -
1983 - Mercedes 300SD - Veggie experiment car "Casper"
2006 - Toyota Sienna - Mine :-( Hey, it's a comapny car!
 
Location: New England | Registered: 16 July 2005Reply With QuoteEdit or Delete MessageReport This Post
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quote:
Originally posted by Jon Heron:
Carl,
No this is incorrect. The start caps on an AC motor are not polarized(+ or -) If a DC cap is used you will be in for a big surprise... BANG.!!!
Once the motor starts turning the Start Capacitor has no effect whatsoever... Its strictly to start the motor.
In laymen terms the capacitor provides a delay in the power given to one of the windings. This delay causes the magnetic forces of the motor to
be unbalanced and the motor then starts to turn in the direction of the weakest pole.
Jon


Aiiyyyeee...

Sorry Jon. I meant this:

quote:
Most smaller, single phase motors usually have a permanent magnet armature that is pushed / pulled around by the rotating inductive field produced by the stator (outside) windings. The inductive field rotates simply as a result of the positive / negative alternations of the 60HZ AC current flowing through the windings. The problem is that when the voltage is applied, the 60HZ is applied immediately, the rotation of the field through the windings begins immediately, and the armature has no chance to react (or catch up, as it were) to the field.

The start cap provides that electrical "push" to get the motor rotation started. It does this by creating a current to voltage lag in the seperate start windings of the motor. Since this current builds up slower, the armature has time to react to the rotating field as it builds up, and to begin rotating with the field. Once the motor is very close to it's rated speed, a centrifugal switch disconnects the start cap and start windings from the circuit. Watching a single phase motor starting you can see that this all happens very quickly.

Without a start cap (such as when one burns up) when the voltage is applied, the motor will just sit and hum. But if you were to grab the shaft and give it a spin, the motor would (usually) start and run normally.


Sorry, I didn't mean a DC cap. The Vodka is kicking in.... methanol exposure is treated though. Roll Eyes


.

C.


Pump and Heater controllers are a must have. (ask Tilly why)
2006 - Jeep Liberty CRD - Wife drives -
1983 - Mercedes 300SD - Veggie experiment car "Casper"
2006 - Toyota Sienna - Mine :-( Hey, it's a comapny car!
 
Location: New England | Registered: 16 July 2005Reply With QuoteEdit or Delete MessageReport This Post
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Hello Carl

Dhill last posted to this forum 26 Dec. 2007 so he was alive at that point. I never heard him talk about any concerns. He also did not wash his biodiesel and at times he said that he would make biodiesel this morning and have it in the car this afternoon.

Yes, Steve has a Canoe Paddle processor that is "Fumeless". I have not followed it's development since he left this forum.



Having a few beers is always a good idea.


Saint Tilly



 
Location: ลึก ประเทศอินเดีย | Registered: 03 March 2001Reply With QuoteEdit or Delete MessageReport This Post
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