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I'm working on my second batch of biodiesel right now (it's cooling in the processor). My first one looked milky after I used my clear water pump to start drying it (after washing it six times and having the last two come out clear). When I titrated it, the result came out at 0.5. Three times.

A few questions for the experienced:

- Is 0.5 a realistic result, or is my test result likely off?
- How long should I mix the oil / methoxide? I had done four hours at 130F.
- If I can't get the biodiesel clean, can I somehow reprocess it?
- What happens if you put more KOH in your methanol than the titration calls for?
 
Location: Hudson Valley, NY | Registered: 11 April 2007Report This Post
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A titration of .5 seams low. The oil I use varies between 2.3-2.8. .5 would be hardly used oil. I mix between 1 and 2 hours at ~140 degrees. That will include 20-30 minutes to mix in the methoxide. You can reprocess to salvage the batch. search reprocessing on this forum. I use NaOH but others here claim KOH can be over used without negative effect.
 
Location: Shelbyville Tennessee | Registered: 06 November 2005Report This Post
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My oil titrates between .5 and 1.2., KOH. Usually under1.

How often do they change the oil? If it is more than once a week, it can be .5.

Andrew


Andrew

http://biodieselcommunity.org
03 Dodge 2500 B100 homebrew
79 Rabbit B100 homebrew
 
Location: Oakland | Registered: 27 February 2006Report This Post
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